4-甲氧基-2,6-二甲基苯甲醛合成路线 （共 29 条）
反应条件
1: hydroxylamine
2: NaOBr
3: (C2H5O)3P
View Scheme
参考文献
Kubota, Tanekazu; Hiramatsu, Sadaaki; Kano, Kenji; Uno, Bunji; Miyazaki, Hiroshi
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3830 - 3839
反应条件
1: N2H4+H2O; KOH; diethylene glycol
2: POCl3
3: N2H4+H2O; KOH; diethylene glycol
4: POCl3
5: N2H4+H2O; KOH; diethylene glycol
View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
1: N2H4+H2O; KOH; diethylene glycol
2: POCl3
3: N2H4+H2O; KOH; diethylene glycol
4: POCl3
5: N2H4+H2O; KOH; diethylene glycol
View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
1: N2H4+H2O; KOH; diethylene glycol
2: POCl3
3: N2H4+H2O; KOH; diethylene glycol
4: POCl3
View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
1: 1.) LiAlH4, 2.) aq. NaOH
2: 92 percent / pyridine
View Scheme
参考文献
Nakatani, Munehiro; Takahashi, Kimi; Watanabe, Sumie; Shintoku, Atsuko; Hase, Tsunao
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 6 p. 1510 - 1514
反应条件
1: N2H4+H2O; KOH; diethylene glycol
2: POCl3
3: N2H4+H2O; KOH; diethylene glycol
4: pyridine hydrochloride
View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
1: NaBH4 / methanol / 0 °C
2: 73 percent / PPh3; CBr4 / Pd2(dba)3 / CH2Cl2 / 0.5 h / 0 - 20 °C
View Scheme
参考文献
Srikrishna; Ravi Kumar; Padmavathi
Synlett, 2002 , # 11 p. 1907 - 1909
反应条件
nitric acid
T=80°C; zuletzt Erwaermen auf Siedetemperatur;
参考文献
Wilds; Djerassi
Journal of the American Chemical Society, 1946 , vol. 68, p. 1862
反应条件
T=80°C; und anschliessendes 1/4-stdg.Erhitzen auf Siedetemperatur;
参考文献
Wilds; Djerassi
Journal of the American Chemical Society, 1946 , vol. 68, p. 1862
