反应条件
1: 85 percent / Na, NH3 / tetrahydrofuran / 1.25 h / -78 °C
2: 72 percent / 4A molecular sieves, p-TSA / CH2Cl2 / 24 h / 20 °C
3: 99 percent / DIBAL / CH2Cl2; hexane / 5 h / Ambient temperature
4: 100 percent / NMO, TPAP / CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
Kim, Kyungjin; Boyd, Vincent A.; Sobti, Aditya; Sulikowski, Gary A.
Israel Journal of Chemistry, 1997 , vol. 37, # 1 p. 3 - 22
