1-(重氮基甲基)-4-硝基苯合成路线 （共 17 条）
反应条件
1: With oxalyl dichloride; dimethyl sulfoxide
Swern oxidation; Inert atmosphere;
2: With triethylamine
Swern oxidation;
参考文献
Moebius, David C.; Kingsbury, Jason S.
Journal of the American Chemical Society, 2009 , vol. 131, p. 878 - 879
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in benzene
T=65 - 70°C; 2 h; Yield given;
参考文献
Wulfman, David S.; Yousefian, Shahram; White, Jon M
Synthetic Communications, 1988 , vol. 18, # 18 p. 2349 - 2352
反应条件
1: 94 percent / N2H4
2: 84 percent / Pb(OAc)4, tetramethylguanidine / dimethylformamide / -78 °C
View Scheme
参考文献
Holton, Terrence L.; Shechter, Harold
Journal of Organic Chemistry, 1995 , vol. 60, # 15 p. 4725 - 4729
反应条件
scandium tris(trifluoromethanesulfonate) in toluene
T=-20°C; 0.166667 h; Inert atmosphere;
参考文献
Wommack, Andrew J.; Kingsbury, Jason S.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10573 - 10587
反应条件
sulfur dioxide
T=20°C; 1 h;
参考文献
Tanabe,T.; Nagai,T.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 1459 - 1463
反应条件
in chloroform; triethylamine
T=20°C; 24 h;
参考文献
Martin, Hans-Dieter; Iden, Ruediger; Mais, Franz-Josef; Kleefeld, Gerd; Steigel, Alois; et al.
Tetrahedron Letters, 1983 , vol. 24, # 49 p. 5469 - 5472
反应条件
tetrafluoroboric acid in dichloromethane
0.166667 h;
参考文献
Takadate, Akira; Tahara, Tsutom; Goya, Shujiro
Synthesis, 1983 , # 10 p. 806 - 807
