1-甲基-1H-咪唑-4,5-二甲腈合成路线 （共 18 条）
反应条件
sodium hydrogencarbonate in water
参考文献
Bures, Filip; Kulhanek, Jiri; Mikysek, Tomas; Ludvik, Jiri; Lokaj, Jan
Tetrahedron Letters, 2010 , vol. 51, # 15 p. 2055 - 2058
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Corelli; Summa; Brogi; Monteagudo; Botta
Journal of Organic Chemistry, 1995 , vol. 60, # 7 p. 2008 - 2015
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-80°C; 0.5 h;
参考文献
Apen, Paul G.; Rasmussen, Paul G.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1091 - 1095
反应条件
1: 4,5-dicyanoimidazole With potassium hydroxide in dimethyl sulfoxide T=20°C; 5 h; 2: methyl iodide in dimethyl sulfoxide T=20 - 50°C;
参考文献
Chemistry - A European Journal, , vol. 16, # 13 p. 3983 - 3993
参考文献
Johnson
Synthesis, 1991 , # 1 p. 75 - 78
参考文献
Johnson
Synthesis, 1991 , # 1 p. 75 - 78
反应条件
in pyridine 6 h; Heating;
参考文献
El Borai, M.; Hassenein, M.
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 853 - 856
反应条件
T=70 - 100°C; 3 h; other orthoesters; also with 4,5-dicyanoimidazole;
参考文献
Johnson
Synthesis, 1991 , # 1 p. 75 - 78
反应条件
in tetrahydrofuran T=-80°C; other 4,5-dicyanoimidazole, var. temp. and amount of lithiating agent; Product distribution;
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 5 p. 1091 - 1095
参考文献
Bulletin de la Societe Chimique de France, , vol. 132, p. 943 - 951
