N-叔丁基=4-甲氧基苯甲酰胺合成路线 (共 29 条)
反应条件
water; sodium acetate in acetonitrile
T=0°C; 1.16667 h; Inert atmosphere;
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: US6384033 B1, 2002 ;
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=110°C; 15 h;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
potassium permanganate; tetrabutyl-ammonium chloride in dichloromethane; water
24 h; Ambient temperaturepH 4.1;
参考文献
Christensen, Dorthe; Joergensen, Karl Anker
Journal of Organic Chemistry, 1989 , vol. 54, # 1 p. 126 - 131
反应条件
pyridine; triethylamine
T=70°C; 26 h;
参考文献
Burhardt, Mia N.; Taaning, Rolf H.; Skrydstrup, Troels
Organic Letters, 2013 , vol. 15, # 4 p. 948 - 951
反应条件
acetic acid; sodium nitrite in water; acetonitrile
T=0 - 20°C; 3 h; Inert atmosphere;
参考文献
Basavanag, Unnamatla M. V.; Dos Santos, Aurelie; El Kaim, Laurent; Gamez-Montano, Rocio; Grimaud, Laurence
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7194 - 7197
Angew. Chem., 2013 , vol. 125, # 28 p. 7335 - 7338,4
反应条件
oxygen; isovaleraldehyde in dichloromethane
T=0°C; 1.5 h;
参考文献
Martiny, Lars; Joergensen, Karl Anker
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 6 p. 699 - 704
反应条件
potassium permanganate in water; acetonitrile
T=50°C; 0.5 h; other conditions: other solvents, other reaction time, other temperature; MechanismRate constantProduct distribution;
参考文献
Larsen, Jan; Jorgensen, Karl Anker; Christensen, Dorthe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1187 - 1190
反应条件
DBU; 5-hydro-3-oxaoctafluoropentanesulfonyl fluoride in dichloromethane
T=20°C; 37 h; Reflux;
参考文献
Yan, Zhaohua; Tian, Weisheng; Zeng, Fanrong; Dai, Yanfeng
Tetrahedron Letters, 2009 , vol. 50, # 23 p. 2727 - 2729
反应条件
1: ethyl tribromoacetate; triphenylphosphine / CH2Cl2 / 3 h / 20 °C
2: Et3N / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Kang, Dong Ho; Joo, Tae Young; Lee, Eun Hwa; Chaysripongkul, Skaydaw; Chavasiri, Warinthorn; Jang, Doo Ok
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5693 - 5696