1-叔丁氧羰基-4-[(甲磺酰基)甲基]哌啶合成路线 （共 5 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C; 12.5 h;
参考文献
CHONG KUN DANG PHARMACEUTICAL CORP.; LEE, ChangSik; JANG, TaegSu; CHOI, DaeKyu; KO, MoonSung; KIM, DoHoon; KIM, SoYoung; MIN, JaeKi; KIM, WooSik; LIM, YoungTae
Patent: WO2013/187646 A1, 2013 ;
Location in patent: Page/Page column 60; 61 ;
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0 - 20°C;
参考文献
F. HOFFMANN-LA ROCHE AG
Patent: WO2009/47161 A1, 2009 ;
Location in patent: Page/Page column 73 ;
反应条件
1: dichloromethane / 3 h / 20 °C / |Cooling with ice 2: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C View Scheme
参考文献
CHONG KUN DANG PHARMACEUTICAL CORP.; LEE, ChangSik; JANG, TaegSu; CHOI, DaeKyu; KO, MoonSung; KIM, DoHoon; KIM, SoYoung; MIN, JaeKi; KIM, WooSik; LIM, YoungTae
Patent: WO2013/187646 A1, 2013 ;
反应条件
1: dichloromethane / 3 h / 20 °C / |Cooling with ice 2: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C View Scheme
参考文献
CHONG KUN DANG PHARMACEUTICAL CORP.; LEE, ChangSik; JANG, TaegSu; CHOI, DaeKyu; KO, MoonSung; KIM, DoHoon; KIM, SoYoung; MIN, JaeKi; KIM, WooSik; LIM, YoungTae
Patent: WO2013/187646 A1, 2013 ;
反应条件
hydrogenchloride in 1,4-dioxane T=0 - 20°C;
参考文献
F. HOFFMANN-LA ROCHE AG
Patent: WO2009/47161 A1, 2009 ;
Location in patent: Page/Page column 73 ;
