1: 1,3-dimethoxy benzene With n-butyllithium in tetrahydrofuran; hexane
T=0°C; 1 h;
2: 2-iodo-1,3-dimethoxybenzene With copper(l) iodide in tetrahydrofuran; pyridine; hexane
72 h; Heating; Further stages.;
参考文献
Govender, Sameshnee; Mmutlane, Edwin M.; Van Otterlo, Willem A. L.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 15 p. 2433 - 2440
1: acetic acid; tin (II)-chloride; hydrogen chloride
2: Diazotization
3: copper-powder / 130 - 190 °C
View Scheme
参考文献
Simada; Hata
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1939 , vol. 35, p. 365,369
Chem. Zentralbl., 1939 , vol. 110, # I p. 4188
Simada; Hata
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1939 , vol. 35, p. 365,369
Chem. Zentralbl., 1939 , vol. 110, # I p. 4188