N-Boc-4,7,10-三氧杂-1,13-十三烷二胺合成路线 (共 7 条)
参考文献
Sadhu, Kalyan K.; Mizukami, Shin; Watanabe, Shuji; Kikuchi, Kazuya
Chemical Communications, 2010 , vol. 46, # 39 p. 7403 - 7405
反应条件
in dichloromethane T=20°C; 16 h;
参考文献
WO2008/75192 A2, ;
Page/Page column 61-62 ;
反应条件
in dichloromethane T=20°C; 6 h;
参考文献
US2008/221343 A1, ;
Page/Page column 9 ;
反应条件
in chloroform-d1 T=25°C; 2 h; Irradiation; Product distributionKinetics; Further Variations:Solventsreaction times, UV wavelengths;
参考文献
Piggott, Andrew M.; Karuso, Peter
Tetrahedron Letters, 2005 , vol. 46, # 47 p. 8241 - 8244
反应条件
in ethanol 20 h; Reflux;
参考文献
Renaud De La Faverie, Amandine; Hamon, Florian; Di Primo, Carmelo; Largy, Eric; Dausse, Eric; Delaurire, Laurence; Landras-Guetta, Corinne; Toulme, Jean-Jacques; Teulade-Fichou, Marie-Paule; Mergny, Jean-Louis
Biochimie, 2011 , vol. 93, # 8 p. 1357 - 1367
反应条件
1: triethylamine / dichloromethane / 1 h / 20 °C 2: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C 3: sodium hydroxide View Scheme
参考文献
Pulido, Daniel; Albericio, Fernando; Royo, Miriam
Organic Letters, 2014 , vol. 16, # 5 p. 1318 - 1321
反应条件
pyridine in dichloromethane; acetonitrile T=20°C; 3.5 h;
参考文献
Trester-Zedlitz, Michelle; Kamada, Katsuhiko; Burley, Stephen K.; Fenyoe, David; Chait, Brian T.; Muir, Tom W.
Journal of the American Chemical Society, 2003 , vol. 125, # 9 p. 2416 - 2425