4-(4,4,5,5-四甲基-1,3,2-二氧硼戊环-2-基)苯甲酸乙酯合成路线 （共 25 条）
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: 4-bromo-benzoic acid ethyl ester in ethylene glycol dimethyl ether T=30°C; 1 h;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
反应条件
(pentamethylcyclopentadienyl)Rh(.eta.4-hexamethylbenzene) T=150°C; 1 h; Title compound not separated from byproducts.;
参考文献
Journal of the American Chemical Society, , vol. 122, # 51 p. 12868 - 12869
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine in 1,4-dioxane T=80°C; Product distribution;
参考文献
Murata, Miki; Watanabe, Shinji; Masuda, Yuzuru
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6458 - 6459
反应条件
in tetrahydrofuran T=20°C;
参考文献
Chemical Communications, , # 35 p. 3667 - 3669
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride in 1,4-dioxane T=100°C; borylation; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 164 - 168
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in N,N-dimethyl-formamide T=80°C; 2 h; Inert atmosphere;
参考文献
Archives of Pharmacal Research, , vol. 33, # 12 p. 1919 - 1926
反应条件
1,1'-bis-(di-tert-butylphosphino)ferrocene; triethylamine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane T=100°C; 24 h; Inert atmosphere;
参考文献
Chemistry Letters, , vol. 40, # 9 p. 962 - 963
反应条件
hydrogenchloride in water T=20°C; 15 h;
参考文献
Heterocycles, , vol. 88, # 1 p. 193 - 199
反应条件
1: triethylamine / dichloromethane 2: potassium acetate / tert-butyl alcohol / 2 h / 90 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 17, # 25 p. 6913 - 6917
反应条件
1: sulfuric acid / 4 h / Reflux 2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere View Scheme
参考文献
Archives of Pharmacal Research, , vol. 33, # 12 p. 1919 - 1926
