4-(4,4,5,5-四甲基-1,3,2-二氧硼戊环-2-基)苯甲酸乙酯合成路线 （共 25 条）
反应条件
1: triethylamine; Pd0(tris(tert-butyl)phosphine)2 / toluene / 3 h / 80 °C / |Sealed tube 2: hydrogenchloride / water / 15 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 88, # 1 p. 193 - 199
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate T=20 - 100°C; Suzuki-Miyaura reaction; Inert atmosphere;
参考文献
Gurung, Santosh K.; Kim, Soo Bae; Park, Haeil
Archives of Pharmacal Research, 2010 , vol. 33, # 12 p. 1919 - 1926
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in N,N-dimethyl-formamide T=90°C; Suzuki-Miyaura coupling; 12 h; Inert atmosphere;
参考文献
Mo, Fanyang; Jiang, Yubo; Qiu, Di; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2010 , vol. 49, # 10 p. 1846 - 1849
反应条件
1: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 20 - 100 °C / Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux; Cooling with ice 3: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux View Scheme
参考文献
Gurung, Santosh K.; Kim, Soo Bae; Park, Haeil
Archives of Pharmacal Research, 2010 , vol. 33, # 12 p. 1919 - 1926
反应条件
1: potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 20 - 100 °C / Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux; Cooling with ice View Scheme
参考文献
Gurung, Santosh K.; Kim, Soo Bae; Park, Haeil
Archives of Pharmacal Research, 2010 , vol. 33, # 12 p. 1919 - 1926
