1-环己基-2-亚甲基氮丙啶合成路线 (共 3 条)
反应条件
1: 86 percent / K2CO3 / tetrahydrofuran / 31 h / Heating 2: 78 percent / NaNH2 / liquid ammonia / 3 h View Scheme
参考文献
Pan, Bin; Wang, Chunxiang; Wang, Dongping; Wu, Fan; Wan, Boshun
Chemical Communications, 2013 , vol. 49, # 44 p. 5073 - 5075
反应条件
1: With copper(l) iodide; boron trifluoride diethyl etherate in tetrahydrofuran T=-30 - 0°C; Ring cleavage; 2: in tetrahydrofuran Hydrolysis; Further stages.;
参考文献
Hayes; Shipman; Twin
Chemical Communications, 2000 , # 18 p. 1791 - 1792
反应条件
copper(l) iodide; boron trifluoride diethyl etherate in tetrahydrofuran T=-30 - 0°C; 1 h;
参考文献
Hayes, Jerome F.; Shipman, Michael; Twin, Heather
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 935 - 942