(E)-2-丁烯-1,4-二醇二(甲烷磺酸酯)合成路线 （共 7 条）
反应条件
potassium hydroxide; triethylamine in benzene
参考文献
Hudson,R.F.; Withey,R.J.
Journal of the Chemical Society [Section] B: Physical Organic, 1966 , p. 237 - 240
反应条件
in dichloromethane Ambient temperature;
参考文献
Ding, Zhaozhong; Tufariello, Joseph J.
Synthetic Communications, 1990 , vol. 20, # 2 p. 227 - 230
反应条件
calcium chloride in dimethyl sulfoxide 3 h; Ambient temperature;
参考文献
Altamura, Maria; Perrotta, Enzo
Journal of Organic Chemistry, 1993 , vol. 58, # 1 p. 272 - 274
反应条件
hydrogenchloride; sodium hydride
1.) THF, DMF, rt, 12 h, 2.) THF, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Park, Kyung-Ho; Olmstead, Marilyn M.; Kurth, Mark J.
Journal of Organic Chemistry, 1998 , vol. 63, # 19 p. 6579 - 6585
反应条件
sodium hydroxide in ethanol; water
参考文献
Hudson,R.F.; Withey,R.J.
Journal of the Chemical Society [Section] B: Physical Organic, 1966 , p. 237 - 240
反应条件
in dichloromethane
Ambient temperature;
参考文献
Ding, Zhaozhong; Tufariello, Joseph J.
Synthetic Communications, 1990 , vol. 20, # 2 p. 227 - 230
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide)
T=20°C;
参考文献
Eisai Co., Ltd.
Patent: EP1375496 A1, 2004 ;
Location in patent: Page 41 ;
