3,4,5,6-四氯邻苯二甲腈合成路线 (共 25 条)
反应条件
ammonia; oxygen; vanadium-tin oxide T=330 - 360°C; 8.33333E-05 h; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Shapovalov, A. A.; Zhalgasbaeva, G. Sh.; Sembaev, D. Kh.; Suvorov, B. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1140 - 1143
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1260 - 1264
反应条件
ammonia; oxygen; vanadium-tin oxide T=330 - 360°C; 8.33333E-05 h; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Shapovalov, A. A.; Zhalgasbaeva, G. Sh.; Sembaev, D. Kh.; Suvorov, B. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1140 - 1143
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1260 - 1264
反应条件
ammonia; oxygen; vanadium-tin oxide T=375 - 405°C; 8.33333E-05 h; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Shapovalov, A. A.; Zhalgasbaeva, G. Sh.; Sembaev, D. Kh.; Suvorov, B. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1140 - 1143
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1260 - 1264
反应条件
ammonia; oxygen; vanadium-tin oxide T=375 - 405°C; 8.33333E-05 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shapovalov, A. A.; Zhalgasbaeva, G. Sh.; Sembaev, D. Kh.; Suvorov, B. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1140 - 1143
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1260 - 1264
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in diethyl ether; chloroform 24 h; Heating;
参考文献
Synthetic Communications, , vol. 15, # 6 p. 479 - 484
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 125 - 129
反应条件
ammonia; oxygen; vanadium-tin oxide T=375 - 405°C; 8.33333E-05 h; other temperature,; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 6 p. 1140 - 1143
Zhurnal Organicheskoi Khimii, , vol. 23, # 6 p. 1260 - 1264
反应条件
sodium hydroxide T=270°C; 16 h;
参考文献
Nippon Shokubai Co., Ltd.
Patent: US6392084 B1, 2002 ;
Location in patent: Page column 16 ;
反应条件
1: dimethyl sulfoxide 2: NH4OH View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
triethylamine in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Volkov; Avramenko; Negrimovskii; Luk'yanets
Russian Journal of General Chemistry, 2007 , vol. 77, # 6 p. 1108 - 1116