3,4,5,6-四氯邻苯二甲腈合成路线 (共 25 条)
反应条件
triethylamine in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Volkov; Avramenko; Negrimovskii; Luk'yanets
Russian Journal of General Chemistry, 2007 , vol. 77, # 6 p. 1108 - 1116
反应条件
1: With lithium; hexan-1-ol 4 h; 2: With acetic acid in acetone
参考文献
Galanin; Shaposhnikov
Russian Journal of General Chemistry, 2012 , vol. 82, # 10 p. 1734 - 1739
Zh. Obshch. Khim., 2012 , vol. 82, # 10 p. 1736 - 1741,6
反应条件
1: dimethyl sulfoxide 2: further solvent(s) View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
1: dimethyl sulfoxide View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
1: dimethyl sulfoxide View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
→
14916-87-11,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-十六氟酞菁铜(II)
反应条件
1: dimethyl sulfoxide View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
potassium fluoride in water
参考文献
Warner-Lambert Company
Patent: US4782180 A1, 1988 ;
反应条件
sodium hydroxide T=270°C; 16 h;
参考文献
Nippon Shokubai Co., Ltd.
Patent: US6392084 B1, 2002 ;
Location in patent: Page column 16 ;
反应条件
potassium fluoride in benzonitrile T=260°C; 18 h;
参考文献
JP2005/112745 A, ;
Page/Page column 8 ;
反应条件
in dimethyl sulfoxide heating to 130-160°C, 0.5-1 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101