(E)-3-(对甲苯磺酰基)丙烯腈合成路线 （共 14 条）
反应条件
1: p-toluenesulfinic acid sodium salt With polystyrene-supported-SeCl in N,N-dimethyl-formamide T=20°C; 6 h; solid-phase reaction; 2: acrylonitrile With 2,2'-azo-bisisobutyronitrile in benzene 20 h; Heating; 3: With dihydrogen peroxide in tetrahydrofuran T=20°C; 2 h;
参考文献
Synlett, , # 12 p. 1913 - 1916
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 0.0833333 h;
参考文献
Journal of Organic Chemistry, , vol. 46, # 16 p. 3249 - 3256
反应条件
triethylamine in dichloromethane 1 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1029 - 1032
反应条件
18-crown-6 ether in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 52, # 19 p. 4265 - 4269
反应条件
1: MCPBA / CH2Cl2 / 0.25 h 2: 56 percent / 18-crown-6 / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 19 p. 4265 - 4269
反应条件
1: 74 percent / CHCl3 / 96 h / Heating 2: 77 percent / m-CPBA / CH2Cl2 / 0.08 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 16 p. 3249 - 3256
反应条件
1: 50 percent / I2 / CH2Cl2 / 48 h / Ambient temperature 2: 87 percent / Et3N / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1029 - 1032
反应条件
1: diethyl ether 2: Et3N / ethyl acetate View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1874 - 1879
反应条件
sodium acetate in 1,4-dioxane; acetic acid
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 13, # 7 p. 1302 - 1305
Zhurnal Organicheskoi Khimii, , vol. 13, # 7 p. 1418 - 1422
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1800 - 1808
