2,2-二甲基-3-庚醇合成路线 （共 14 条）
反应条件
in diethyl ether; hexane 1.) -78 deg C, 1 h, 2.) room temp., 2.5 h;
参考文献
Heathcock, , Clayton H.; Lampe, John
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4330 - 4337
反应条件
chloro-trimethyl-silane; CaH2; zinc(II) chloride in tetrahydrofuran T=40°C; 24 h;
参考文献
Tsuhako, Akiko; He, Jing-Qian; Mihara, Mariko; Saino, Naoko; Okamoto, Sentaro
Tetrahedron Letters, 2007 , vol. 48, # 52 p. 9120 - 9123
反应条件
in tetrahydrofuran; dimethyl-ether T=-110°C;
参考文献
Seyferth, Dietmar; Weinstein, Robert M.; Hui, Richard C.; Wang, Wei-Liang; Archer, Colin M.
Journal of Organic Chemistry, 1992 , vol. 57, # 21 p. 5620 - 5629
反应条件
(.eta.5-C5H5)2Sm; oxonium in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Namy, J. L.; Collin, J.; Zhang, J.; Kagan, H. B.
Journal of Organometallic Chemistry, 1987 , vol. 328, p. 81 - 86
参考文献
Whitmore
Recueil des Travaux Chimiques des Pays-Bas, 1938 , vol. 57, p. 566
Full Text Show Details
Whitmore et al.
Journal of the American Chemical Society, 1938 , vol. 60, p. 2462,2791
参考文献
Whitmore
Recueil des Travaux Chimiques des Pays-Bas, 1938 , vol. 57, p. 566
Full Text Show Details
Whitmore et al.
Journal of the American Chemical Society, 1938 , vol. 60, p. 2462,2791
反应条件
1: diethyl ether; copper (I)-chloride 2: lithium alanate View Scheme
参考文献
Foley et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2779,2280
反应条件
2: diethyl ether View Scheme
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1938 , vol. 60, p. 2462,2791
反应条件
in tetrahydrofuran; dimethyl-ether T=-135°C;
参考文献
Seyferth, Dietmar; Weinstein, Robert M.; Wang, Wei-Liang
Journal of Organic Chemistry, 1983 , vol. 48, # 7 p. 1144 - 1146
参考文献
Colonge; Lagier
Bulletin de la Societe Chimique de France, 1949 , p. 16
