3,5-二甲基-4-庚酮合成路线 (共 13 条)
反应条件
1: With N,N,N',N,-tetramethylethylenediamine in diethyl ether; cyclohexane T=-78°C; 0.166667 h; Inert atmosphere; 2: With methanol-d1 in diethyl ether; cyclohexane T=-78°C; Inert atmosphereMolecular sieve;
参考文献
Organic Letters, , vol. 13, # 3 p. 394 - 397
反应条件
manganese bromide tetrahydrate; lithium hexamethyldisilazane in tetrahydrofuran T=22°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 34, # 46 p. 7395 - 7398
反应条件
in diethyl ether a) RT, 30 min, b) reflux, 30 min;
参考文献
Heterocycles, , vol. 40, # 1 p. 79 - 84
参考文献
Journal of the American Chemical Society, , vol. 95, p. 6876 - 6877
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 177, p. 454
反应条件
Cu-Zn-Mg-Al based catalyst; hydrogen reduced T=249.84°C; Product distribution / selectivity;
参考文献
US7314960 B1, ;
Page/Page column 4-8 ;
反应条件
diethyl ether folgende Hydrolyse;
参考文献
Canadian Journal of Research, Section B: Chemical Sciences, , vol. 27, p. 64
反应条件
diethyl ether; sodium amide
参考文献
Chemische Berichte, , vol. 70, p. 620
Zhurnal Obshchei Khimii, , vol. 7, p. 717
反应条件
(i) Mg, Et2O, (ii) /BRN= 907359/, THF, (iii) H2, Pd-C, MeOH; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 2673 - 2676
反应条件
(i) Mg, Et2O, (ii) /BRN= 1720487/, Cu2I2; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 2673 - 2676