反-2,2-二甲基-3-庚烯合成路线 (共 8 条)
反应条件
CrCl2*DMF in tetrahydrofuran T=25°C; 1 h; var. aldehydes, E-selectivity; Product distribution;
参考文献
Okazoe, Takashi; Takai, Kazuhiko; Utimoto, Kiitiro
Journal of the American Chemical Society, 1987 , vol. 109, # 3 p. 951 - 953
反应条件
lithium hexamethyldisilazane in tetrahydrofuran -78 deg C -> 23 deg C;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 7664
参考文献
Tetrahedron Letters, , vol. 30, # 11 p. 1361 - 1364
反应条件
in diethyl ether T=25°C; 19 h;
参考文献
Tetrahedron, , vol. 40, # 9 p. 1457 - 1468
反应条件
in tetrahydrofuran T=25°C; 2 h; Title compound not separated from byproducts;
参考文献
Synthesis, , # 2 p. 109 - 111
反应条件
in tetrahydrofuran T=25°C; 2 h; Title compound not separated from byproducts;
参考文献
Synthesis, , # 2 p. 109 - 111
反应条件
1: tetrahydrofuran-d8 / 0.02 h / -78 °C 2: -15 °C / time spectrum is from t=0 to 14 h. View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 11 p. 1361 - 1364
反应条件
Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 30, # 11 p. 1361 - 1364