3,4-二甲基-3-己烯合成路线 （共 18 条）
反应条件
ozone; polyethylene T=-77°C; 20 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 383 - 389
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
反应条件
ammonia; sodium in diethyl ether
1.25 h;
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
反应条件
ammonia; sodium in diethyl ether
1.25 h;
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
反应条件
ammonia; sodium in diethyl ether
1.25 h;
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
反应条件
ammonia; sodium in diethyl ether
1.25 h;
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
反应条件
1: 80 percent / benzene; diethyl ether / 2 - 20 °C
2: 62 percent / sodium in ammonia, ammonium chloride / diethyl ether / 0.33 h
3: toluene-p-sulphonic acid / benzene / Heating
4: LDA / diethyl ether / 11 h / 20 °C
View Scheme
参考文献
Brown, Michael D.; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 817 - 822
反应条件
1: 71 percent / MgBr2 / diethyl ether / Heating
2: 62 percent / sodium in ammonia, ammonium chloride / diethyl ether / 0.33 h
3: toluene-p-sulphonic acid / benzene / Heating
4: LDA / diethyl ether / 11 h / 20 °C
View Scheme
参考文献
Brown, Michael D.; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 817 - 822
反应条件
2: triethyl phosphite / 100 h / Heating
View Scheme
参考文献
Quast, Helmut; Fuss, Andreas; Heublein, Alfred; Jakobi, Harald; Seiferling, Bernhard
Chemische Berichte, 1991 , vol. 124, # 11 p. 2545 - 2554
