3,4-二甲基-3-己烯合成路线 （共 18 条）
反应条件
tert.-butyl lithium
1.) Et2O, pentane, -80 deg C to 20 deg C; 2.) Et2O, pentane, -40 deg C to r.t.; Yield given. Multistep reaction;
参考文献
Maercker; Girreser
Tetrahedron, 1994 , vol. 50, # 27 p. 8019 - 8034
反应条件
lithium
1.) Et2O, r.t.; 2.) Et2O, -40 deg C to r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Maercker; Girreser
Tetrahedron, 1994 , vol. 50, # 27 p. 8019 - 8034
参考文献
Lewina et al.
Zhurnal Obshchei Khimii, 1953 , vol. 23, p. 729,733; engl. Ausg. S. 759, 764
反应条件
lithium; dimethyl sulfate
1.) Et2O, r.t., 664 h; 2.) Et2O, -40 deg C to r.t.; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Maercker; Girreser
Tetrahedron, 1994 , vol. 50, # 27 p. 8019 - 8034
反应条件
T=90°C; Irradiation;
参考文献
Quast, Helmut; Fuss, Andreas; Heublein, Alfred; Jakobi, Harald; Seiferling, Bernhard
Chemische Berichte, 1991 , vol. 124, # 11 p. 2545 - 2554
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
反应条件
T=200°C; Product distribution; Further Variations:Temperatures;
参考文献
Breton, Gary W.; Nickerson, Justine E.; Greene, Anna M.; Oliver, Lindsey H.
Organic Letters, 2007 , vol. 9, # 16 p. 3005 - 3008
反应条件
T=714.4°C; further temperatures; ΔH(exit.); ΔS(exit.); Rate constantThermodynamic data;
参考文献
Doering, William v. E.; Roth, Wolfgang R.; Bauer, Frank; Breuckmann, Rolf; Ebbrecht, Thomas; at al.
Chemische Berichte, 1989 , vol. 122, p. 1263 - 1276
