2,2-二甲基-5-己烯-3-醇合成路线 （共 22 条）
反应条件
InI3; dimethylphenylsilane in dichloromethane
T=20°C; 1.66667 h; Inert atmosphere; chemoselective reaction;
参考文献
Nishimoto, Yoshihiro; Inamoto, Yoshihiro; Saito, Takahiro; Yasuda, Makoto; Baba, Akio
European Journal of Organic Chemistry, 2010 , # 18 p. 3382 - 3386
反应条件
in dichloromethane; water
T=20°C; Addition; 16 h;
参考文献
Gable; Shanmugham; White
Canadian Journal of Chemistry, 2000 , vol. 78, # 6 p. 704 - 707
反应条件
tin(ll) chloride in acetonitrile
1 h;
参考文献
Yasuda, Makoto; Sugawa, Yoshihiro; Yamamoto, Akihiro; Shibata, Ikuya; Baba, Akio
Tetrahedron Letters, 1996 , vol. 37, # 33 p. 5951 - 5954
反应条件
montmorillonite-enwrapped copper
T=45°C; Sakurai-Hosomi reaction; 1 h; Title compound not separated from byproducts;
参考文献
Kawabata, Tomonori; Kato, Masaki; Mizugaki, Tomoo; Ebitani, Kohki; Kaneda, Kiyotomi
Chemistry - A European Journal, 2005 , vol. 11, # 1 p. 288 - 297
反应条件
indium in water
17 h; Ambient temperature;
参考文献
Chen, Dong-Li; Li, Chao-Jun
Tetrahedron Letters, 1996 , vol. 37, # 3 p. 295 - 298
反应条件
di-n-butyldichlorostannane
58 h; Ambient temperature; Yields of byproduct given;
参考文献
Whitesell, James K.; Apodaca, Richard
Tetrahedron Letters, 1996 , vol. 37, # 23 p. 3955 - 3958
反应条件
(i) pentane, (ii) H2NCH2CH2OH; Multistep reaction;
参考文献
Kramer,G.W.; Brown,H.C.
Journal of Organic Chemistry, 1977 , vol. 42, p. 2292 - 2299
参考文献
Harayama, Hiroto; Abe, Atsuhiro; Sakado, Tomonori; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Journal of Organic Chemistry, 1997 , vol. 62, # 7 p. 2113 - 2122
反应条件
(i) (oxidation), (ii) /BRN= 3536275/; Multistep reaction;
参考文献
Chuchani,G. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1973 , p. 1961 - 1963
反应条件
(i) (+)-2-exo,-3-exo-dihydroxy-3-endo-phenyl-bornane, THF, (ii) /BRN= 506060/, n-hexane, (iii) (HOCH2CH2)3N; Multistep reaction;
参考文献
Herold,T.; Hoffmann,R.W.
Angewandte Chemie, 1978 , vol. 90, p. 822 - 823
