2,2-二甲基-5-己烯-3-醇合成路线 (共 22 条)
反应条件
Jone's reagent in diethyl ether
T=0 - 20°C;
参考文献
Zhu, Liping; Yu, Hongmei; Xu, Zhaoqing; Jiang, Xianxing; Lin, Li; Wang, Rui
Organic Letters, 2014 , vol. 16, # 6 p. 1562 - 1565
反应条件
1: Jone's reagent / diethyl ether / 0 - 20 °C
2: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C
3: triethylamine / dichloromethane / 0 °C
4: copper(I) bromide / toluene / 120 °C / |Inert atmosphere
View Scheme
参考文献
Du, Wei; Zhao, Mi-Na; Ren, Zhi-Hui; Wang, Yao-Yu; Guan, Zheng-Hui
Chemical Communications, 2014 , vol. 50, # 56 p. 7437 - 7439