2,3-二甲基-5-己烯-3-醇合成路线 (共 11 条)
反应条件
Montmorillonite K10; water in dichloromethane T=20°C; Inert atmosphere;
参考文献
Nowrouzi, Farhad; Thadani, Avinash N.; Batey, Robert A.
Organic Letters, 2009 , vol. 11, # 12 p. 2631 - 2634
反应条件
ammonium chloride; tin(ll) chloride; zinc(II) iodide in water T=30°C; 17 h;
参考文献
Wang, Jun; Yuan, Gu
Synthetic Communications, 2006 , vol. 36, # 3 p. 401 - 405
反应条件
tin(ll) chloride in acetonitrile 2 h;
参考文献
Yasuda, Makoto; Sugawa, Yoshihiro; Yamamoto, Akihiro; Shibata, Ikuya; Baba, Akio
Tetrahedron Letters, 1996 , vol. 37, # 33 p. 5951 - 5954
反应条件
in diethyl ether 1 h; Heating;
参考文献
Curry, Michael J.; Stevens, D.R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1756 - 1760
参考文献
Wagner jun.
Chem. Zentralbl., 1901 , vol. 72, # I p. 668
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Schryver
Journal of the Chemical Society, 1893 , vol. 63, p. 1336
参考文献
Schryver
Journal of the Chemical Society, 1893 , vol. 63, p. 1336
反应条件
(i) Mg, (ii) /BRN= 1071238/; Multistep reaction;
参考文献
Dreyfuss,M.P.
Journal of Organic Chemistry, 1963 , vol. 28, p. 3269 - 3272
反应条件
in neat (no solvent) byproducts: methyl isopropyl ketone; 220°C, 10 h (distn. off of ketone); distn. (reduced pressure);
参考文献
Tagliavini et al.
Inorganica Chimica Acta, 1978 , vol. 26, p. L41
参考文献
Journal of Organometallic Chemistry, , vol. 162, p. 37 - 44
反应条件
in neat (no solvent) byproducts: methyl isopropyl ketone; 220°C, 10 h (distn. off of ketone); distn. (reduced pressure);
参考文献
Tagliavini et al.
Inorganica Chimica Acta, 1978 , vol. 26, p. L41