1-(4-氯苯基)-乙酮肟合成路线 （共 37 条）
反应条件
sodium hydroxide in nitromethane; dimethyl sulfoxide T=110°C; 16 h; Schlenk technique;
参考文献
Sha, Qiang; Wei, Yunyang
Tetrahedron, 2013 , vol. 69, # 19 p. 3829 - 3835
反应条件
EtO-NO; TEAB in benzene 22 h; Ambient temperature;
参考文献
Okamoto, Tadashi; Kobayashi, Kenji; Oka, Shinzaburo; Tanimoto, Shigeo
Journal of Organic Chemistry, 1988 , vol. 53, # 21 p. 4897 - 4901
反应条件
hydroxylamine hydrochloride; silica gel 0.116667 h;
参考文献
Hajipour; Mohammadpoor-Baltork; Nikbaghat; Imanzadeh
Synthetic Communications, 1999 , vol. 29, # 10 p. 1697 - 1701
反应条件
hydrazine hydrate in ethanol 6 h; Heating;
参考文献
Danagulyan, G. G.; Balasanyan, N. G.; Terent'ev, P. B.; Zalinyan, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 12 p. 1369 - 1373
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 12 p. 1644 - 1648
反应条件
hydrazine hydrate in ethanol 6 h; Heating;
参考文献
Danagulyan, G. G.; Balasanyan, N. G.; Terent'ev, P. B.; Zalinyan, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 12 p. 1369 - 1373
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 12 p. 1644 - 1648
反应条件
1: ethanol / 3 h 2: 81 percent / dimethylformamide / 5 h / 20 °C 3: N2H4*H2O / ethanol / 6 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 25, # 12 p. 1369 - 1373
Khimiya Geterotsiklicheskikh Soedinenii, , # 12 p. 1644 - 1648
反应条件
1: carbon disulfide; AlCl3 2: water; natrium carbonate; alcohol; hydroxylamine hydrochloride View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 21, p. 67
反应条件
1: With (Ph)2SiH2; silver trifluoromethanesulfonate in tetrahydrofuran T=20°C; 25 h; 2: With hydrogenchloride in tetrahydrofuran; methanol Further stages. Title compound not separated from byproducts.;
参考文献
Takei; Nishibayashi; Ishii; Mizobe; Uemura; Hidai
Chemical Communications, 2001 , # 22 p. 2360 - 2361
反应条件
silica gel; iron(III) chloride in 1,2-dichloro-ethane 5 h; Heating;
参考文献
Khadilkar, Bhushan M.; Upadhyaya, Dharita J.
Synthetic Communications, 2002 , vol. 32, # 12 p. 1867 - 1873
反应条件
potassium hydroxide in dimethyl sulfoxide T=20 - 35°C; Etherification; Alkylation; Hydrolysis; 2.5 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 35, # 11 p. 1581 - 1586
