lithium hydroxide; (DHQD)2PHAL; K2lt;OsO2(OH)4gt; in tert-butyl alcohol T=4°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bruncko, Milan; Schlingloff, Gunther; Barry Sharpless
Angewandte Chemie (International Edition in English), 1997 , vol. 36, # 13-14 p. 1483 - 1486
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反应条件
Boc-(π-Me)-L-His-D-Pro-CSNH-Aib-L-Phe-OMe; triethylamine in toluene T=25°C; 3 h; Resolution of racemate;
参考文献
Chen, Peng; Qu, Jin
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 2994 - 3004