7A-甲基-2,3,5,6,7,7A-六氢-1H-茚-1,5-二酮合成路线 （共 26 条）
反应条件
toluene-4-sulfonic acid; L-proline 1.) CHCl3, rt, 54 h, 2.) benzene, reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 61, # 10 p. 3520 - 3530
反应条件
CHF3O3S*C10H24N2; meta-nitrobenzoic acid T=20°C; 12 h; Neat (no solvent); optical yield given as percent eeenantioselective reaction;
参考文献
Zhou, Pengxin; Zhang, Long; Luo, Sanzhong; Cheng, Jin-Pei
Journal of Organic Chemistry, 2012 , vol. 77, # 5 p. 2526 - 2530
反应条件
toluene-4-sulfonic acid in toluene 5 h; Heating; Title compound not separated from byproducts.;
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 19 p. 3190 - 3200
反应条件
toluene-4-sulfonic acid in benzene 1 h; Heating;
参考文献
Sevillano; Melero; Caballero; Tome; Lelievre; Geering; Crambert; Carron; Medarde; San Feliciano
Journal of Medicinal Chemistry, 2002 , vol. 45, # 1 p. 127 - 136
反应条件
1: With acetic acid in water 2: With R-(+)-proline in N,N-dimethyl-formamide 3: With sulfuric acid in N,N-dimethyl-formamide Further stages.;
参考文献
Molander, Gary A.; Quirmbach, Michael S.; Silva Jr., Luiz F.; Spencer, Keith C.; Balsells, Jaume
Organic Letters, 2001 , vol. 3, # 15 p. 2257 - 2260
反应条件
cultures of curvularia falcata
参考文献
Helvetica Chimica Acta, , vol. 41, p. 1428,1430
反应条件
1: 100 percent / triethylamine / acetonitrile / 20 °C 2: (S)-5,6-dimethyl-2-(pyrrolidin-2-yl)-1H-benzimidazole; TFA / tetrahydrofuran / 48 h / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 1 p. 167 - 177
反应条件
1: 2-methyl-1,3-cyclo-pentanedione With L-proline in dimethyl sulfoxide T=15 - 25°C; 6 h; 2: methyl vinyl ketone in dimethyl sulfoxide T=15 - 25°C; asymmetric Robinson annulation; 145 h; 3: With pyridinium p-toluenesulfonate in benzene 2 h; Heating;
参考文献
Tetrahedron Letters, , vol. 42, # 29 p. 4887 - 4890
反应条件
L-proline in chloroform T=20°C; Hajos-Parrish reaction; 316 h; optical yield given as percent eeenantioselective reaction;
参考文献
de Arriba, Angel L. Fuentes; Simon, Luis; Raposo, Cesar; Alcazar, Victoria; Moran, Joaquin R.
Tetrahedron, 2009 , vol. 65, # 25 p. 4841 - 4845
