alpha,alpha,alpha',alpha',alpha'',alpha''-六甲基苯-1,3,5-三甲醇合成路线 （共 15 条）
反应条件
sulfuric acid T=60°C; 16 h;
参考文献
THE UNIVERSITY OF AKRON; KENNEDY, Joseph P.; ERDODI, Gabor
Patent: WO2012/94246 A1, 2012 ;
Location in patent: Page/Page column 16 ;
反应条件
ethanol; copper oxide-chromium oxide T=225°C; P=110326 Torr; Hydrogenation;
参考文献
Wibaut; Paulis
Recueil des Travaux Chimiques des Pays-Bas, 1958 , vol. 77, p. 792,798
Proceedings of the Koninklijke Nederlandse Akademie van Wetenschappen, Series B: Physical Sciences, 1958 , vol. <B> 61, p. 103,105
反应条件
(((3-hydroxypropyl)carbonylcyclopentadienyl)cobalt)-η4-cyclooctadiene in methanol; water
参考文献
Sigman; Fatland; Eaton
Journal of the American Chemical Society, 1998 , vol. 120, # 20 p. 5130 - 5131
反应条件
sodium sulfite in diethyl ether; water
T=10 - 20°C; pH=6 - 7; 1 h;
参考文献
THE UNIVERSITY OF AKRON; KENNEDY, Joseph P.; ERDODI, Gabor
Patent: WO2012/94246 A1, 2012 ;
Location in patent: Page/Page column 15-16 ;
反应条件
lt;Ni(NCS)(Clt;*gt;C-C(CH3)2(OH))(Ph3P)2gt; in diethylamine
6 h; Heating;
参考文献
Bicev, Peter; Furlani, Anita; Russo, Maria Vittoria
Gazzetta Chimica Italiana, 1980 , vol. 110, # 1 p. 25 - 30
反应条件
bis(acetylacetonate)nickel(II)
T=40°C; 0.666667 h;
参考文献
Ananikov; Zalesskiy; Orlov; Beletskaya
Russian Chemical Bulletin, 2006 , vol. 55, # 11 p. 2109 - 2113
反应条件
{NiBr2(Tri-{n-butyl}-phosphin)2} in hexane
5 h; Heating;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
{NiBr2(Tri-{n-butyl}-phosphin)2} in Petroleum ether
7 h; Heating;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
NiBr2(PPh3)2 in benzene
5 h; Heating;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
{NiBr2(Tri-{n-butyl}-phosphin)2} in Petroleum ether
7 h; Heating; Yields of byproduct given;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
