2-[(4-甲基哌嗪-1-基)甲基]苯胺合成路线 （共 4 条）
反应条件
hydrogen in ethanol T=20°C; P=2068.65 Torr; 1 h;
参考文献
Moore, Terry W.; Sana, Kasinath; Yan, Dan; Thepchatri, Pahk; Ndungu, John M.; Saindane, Manohar T.; Lockwood, Mark A.; Natchus, Michael G.; Liotta, Dennis C.; Plemper, Richard K.; Snyder, James P.; Sun, Aiming
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 197 - 203
反应条件
C52H67ClFeNPPd; caesium carbonate in tetrahydrofuran; water T=80°C; Suzuki-Miyaura cross-coupling; 12 h;
参考文献
Zou, Dapeng; Cui, Hongmeng; Qin, Lijin; Li, Jingya; Wu, Yangjie; Wu, Yusheng
Synlett, 2011 , # 3 art. no. S05710ST, p. 349 - 356
反应条件
1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 20 °C 2: hydrogen / ethanol / 1 h / 20 °C / 2068.65 Torr View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 197 - 203
反应条件
1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 20 °C 2: hydrogen / ethanol / 1 h / 20 °C / 2068.65 Torr View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 197 - 203
