1: With bis (triortho-tolylphosphine)palladium(II) chloride; zinc in tetrahydrofuran; N,N-dimethyl acetamide T=60°C; Condensation; 3 h; 2: With hydrogen; palladium on activated charcoal in tetrahydrofuran T=20°C; Hydrogenolysis; 21 h;
参考文献
Kendall, John T.
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 5 p. 505 - 514
1: With bis (triortho-tolylphosphine)palladium(II) chloride; zinc in tetrahydrofuran; N,N-dimethyl acetamide T=60°C; Condensation; 3 h; 2: With hydrogen; palladium on activated charcoal in tetrahydrofuran T=20°C; Hydrogenolysis; 21 h;
参考文献
Kendall, John T.
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 5 p. 505 - 514
bis (triortho-tolylphosphine)palladium(II) chloride; zinc in tetrahydrofuran; N,N-dimethyl acetamide T=60°C; Condensation; reduction; 3 h; Title compound not separated from byproducts;
参考文献
Kendall, John T.
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 5 p. 505 - 514
1: With copper(l) iodide; diethylamine; bis-triphenylphosphine-palladium(II) chloride T=0 - 25°C; 6 h; 2: With water in ethyl acetate 3: With potassium hydroxide in methanol T=25°C; 1 h;
