1-(3,4-二甲氧基苯基)-2-丙醇合成路线 (共 14 条)
反应条件
thionyl chloride in benzene
20 h; Ambient temperature;
参考文献
Rehse; Behncke; Siemann; Kehr
Archiv der Pharmazie, 1980 , vol. 313, # 3 p. 221 - 229
反应条件
1: 89 percent / HCl gas / dioxane / 1 h / Heating
2: 75 percent / chromium trioxide, 35percent H2SO4 / acetone; H2O / 2 h / Ambient temperature
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参考文献
Gatta; Piazza; Del Giudice; Massotti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 12 p. 942 - 955
反应条件
1: 85 percent / HCl gas / dioxane / 1 h / Heating
2: 54 percent / chromium trioxide, 35percent H2SO4 / acetone; H2O / 2 h / Ambient temperature
3: 68 percent / hydrazin hydrate 98percent / ethanol / 1 h / Heating
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参考文献
Gatta; Piazza; Del Giudice; Massotti
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 12 p. 942 - 955
反应条件
1: CrO3, H2SO4
2: MCPBA
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参考文献
Manitto,P. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1548 - 1551