carbon tetrabromide; triphenylphosphine in dichloromethane T=20°C; 2 h;
参考文献
McAllister, Laura A.; Bechle, Bruce M.; Dounay, Amy B.; Evrard, Edelweiss; Gan, Xinmin; Ghosh, Somraj; Kim, Ji-Young; Parikh, Vinod D.; Tuttle, Jamison B.; Verhoest, Patrick R.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3484 - 3497
1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C 1.2: 0.75 h / 0 °C 2.1: ethanol; SnCl2·2H2O / 70 °C 3.1: hydrogenchloride; acetic acid / water / 1 h / 90 °C View Scheme
