2-(6-甲氧基吡啶-2-基)乙醇合成路线 （共 4 条）
反应条件
n-butyllithium in tetrahydrofuran T=0°C;
参考文献
Brodney, Michael A.; Padwa, Albert
Tetrahedron Letters, 1997 , vol. 38, # 35 p. 6153 - 6156
反应条件
1: With sodium tetrahydroborate; ethanol T=20°C; 2: With water; sodium hydrogencarbonate in ethyl acetate
参考文献
ASTRAZENECA AB
Patent: US2010/331341 A1, 2010 ;
Location in patent: Page/Page column 28 ;
反应条件
1.1: Ag2CO3 / CHCl3 2.1: n-BuLi / tetrahydrofuran / -78 °C 2.2: tetrahydrofuran / -78 - 20 °C View Scheme
参考文献
Brodney, Michael A.; Padwa, Albert
Tetrahedron Letters, 1997 , vol. 38, # 35 p. 6153 - 6156
反应条件
disodium hydrogenphosphate; bromine in methanol; water
T=20°C; 12 h;
参考文献
Forest Laboratories Holdings Limited
Patent: US2007/281918 A1, 2007 ;
Location in patent: Page/Page column 14 ;
US 20070281918 A1
