1,3-二甲基吡咯烷-2-酮合成路线 (共 13 条)
反应条件
1: triethylamine / dichloromethane / 0.5 h / Inert atmosphere 2: 4-(N,N-dimethlyamino)pyridine / dichloromethane / Inert atmosphere 3: dichloromethane / 2 h / Inert atmosphere 4: water; isopropyl alcohol / 37 °C / pH 7.4 / aq. phosphate buffer View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 6 p. 1846 - 1854
反应条件
lithium diisopropyl amide 1) THF, hexane, -78 deg C, 30 min, 2) THF, 1 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 11 p. 1119 - 1124
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 23, p. 1981,1983
Journal of the American Chemical Society, , vol. 63, p. 228,233