反应条件
1: Zn, I2 / tetrahydrofuran / 45 °C
2: 1.) p-TsOH, 2.) 10percent KOH / 1.) benzene, RT, overnight, 2.) ethanediol, 185-190 deg C
3: CH3SO3H / 4 h / 55 - 60 °C
4: 94 percent / NaBH4 / tetrahydrofuran; methanol / 1 h / Ambient temperature
5: 100 percent / p-TsOH / benzene / Ambient temperature
6: o-chloranil / benzene / 72 h / Ambient temperature
View Scheme
参考文献
Bushman, Daniel R.; Grossman, Scott J.; Jerina, Donald M.; Lehr, Roland E.
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3533 - 3544
