反应条件
1.1: diethyl ether; tetrahydrofuran / 0 - 20 °C / |Inert atmosphere
2.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / |Inert atmosphere
2.2: -78 - 20 °C / |Inert atmosphere
3.1: It-Bu2; bis(1,5-cyclooctadiene)nickel (0) / 1,3,5-trimethyl-benzene / 1 h / 130 °C / |Inert atmosphere
View Scheme
参考文献
Hoshimoto, Yoichi; Hayashi, Yukari; Suzuki, Haruka; Ohashi, Masato; Ogoshi, Sensuke
Angewandte Chemie - International Edition, 2012 , vol. 51, # 43 p. 10812 - 10815
Angew. Chem., 2012 , vol. 124, # 43 p. 10970 - 10973,4
