1: 1-bromo-2-(methylthio)benzene With iodine; magnesium in tetrahydrofuran
3.66667 h;
2: glutaric acid anhydride in tetrahydrofuran
T=-40 - 20°C;
参考文献
Kooistra, Floris B.; Knol, Joop; Kastenberg, Fredrik; Popescu, Lacramioara M.; Verhees, Wiljan J. H.; Kroon, Jan M.; Hummelen, Jan C.
Organic Letters, 2007 , vol. 9, # 4 p. 551 - 554