N-(2-甲基-4-甲氧基-5-硝基苯基)乙酰胺合成路线 （共 8 条）
反应条件
trifluoroacetic acid; sodium nitrite T=0 - 20°C; Inert atmosphere;
参考文献
Thompson, Sam; Vallinayagam, Ramakrishnan; Adler, Marc J.; Scott, Richard T.W.; Hamilton, Andrew D.
Tetrahedron, 2012 , vol. 68, # 23 p. 4501 - 4505
反应条件
nitric acid in dichloromethane
参考文献
Zeneca Limited
Patent: US6184225 B2, 2001 ;
反应条件
chloroform; water; nitric acid T=-5°C;
参考文献
MacMillan
Journal of the Chemical Society, 1952 , p. 4019,4021
反应条件
1: potassium permanganate; magnesium sulfate; water 2: aqueous hydrochloric acid View Scheme
参考文献
Dewar
Journal of the Chemical Society, 1944 , p. 619,622
反应条件
potassium permanganate; magnesium sulfate in water T=80°C; 1.5 h; Inert atmosphere;
参考文献
Thompson, Sam; Vallinayagam, Ramakrishnan; Adler, Marc J.; Scott, Richard T.W.; Hamilton, Andrew D.
Tetrahedron, 2012 , vol. 68, # 23 p. 4501 - 4505
反应条件
potassium permanganate in water
参考文献
Zeneca Limited
Patent: US6184225 B2, 2001 ;
反应条件
1: potassium permanganate; magnesium sulfate; water 2: aqueous hydrochloric acid View Scheme
参考文献
Dewar
Journal of the Chemical Society, 1944 , p. 619,622
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MacMillan
Journal of the Chemical Society, 1952 , p. 4019,4021
反应条件
1: aqueous hydrochloric acid
2: Raney nickel; methanol / Hydrogenation
View Scheme
参考文献
MacMillan
Journal of the Chemical Society, 1952 , p. 4019,4021
