2-乙酰氨基-4-硝基-5-甲氧基苯甲酸合成路线 (共 6 条)
反应条件
potassium permanganate; magnesium sulfate in water T=80°C; 1.5 h; Inert atmosphere;
参考文献
Thompson, Sam; Vallinayagam, Ramakrishnan; Adler, Marc J.; Scott, Richard T.W.; Hamilton, Andrew D.
Tetrahedron, 2012 , vol. 68, # 23 p. 4501 - 4505
反应条件
potassium permanganate in water
参考文献
Zeneca Limited
Patent: US6184225 B2, 2001 ;
反应条件
1: acetic acid; nitric acid / -5 °C 2: potassium permanganate; magnesium sulfate; water View Scheme
参考文献
Journal of the Chemical Society, , p. 619,622
Journal of the Chemical Society, , p. 4019,4021
反应条件
1: pyridine / 0 - 20 °C / Inert atmosphere 2: trifluoroacetic acid; sodium nitrite / 0 - 20 °C / Inert atmosphere 3: potassium permanganate; magnesium sulfate / water / 1.5 h / 80 °C / Inert atmosphere View Scheme
参考文献
Tetrahedron, , vol. 68, # 23 p. 4501 - 4505
反应条件
1: 92 percent / aq. HCl / 3 h / Heating 2: 67 percent / 4.5 h / Heating View Scheme
参考文献
Dewar
Journal of the Chemical Society, 1944 , p. 619,622
反应条件
hydrogenchloride Deacetylation; 3 h; Heating;
参考文献
Zeneca Limited
Patent: US6184225 B2, 2001 ;