反应条件
1: isopropyl-triphenyl-phosphonium iodide With sodium hydride in dimethyl sulfoxide; mineral oil T=50°C; Wittig Reaction; 0.75 h; Inert atmosphere; 2: 1,4-cyclohexanedione monoacetal in dimethyl sulfoxide; mineral oil T=50°C; Wittig Reaction; 16.75 h;
参考文献
NEO ONCOLOGY INC.; CHEN, Thomas; LEVIN, Daniel; PUPPALI, Satish; DICKMAN, Daniel, A.
Patent: WO2012/83178 A1, 2012 ;
Location in patent: Page/Page column 35-36 ;