2-(3-溴苯基)苯并[d]噻唑合成路线 （共 9 条）
反应条件
oxygen; carbon in anhydrous xylene
T=50°C; 29 h; Inert atmosphere;
参考文献
Dhayalan, Vasudevan; Hayashi, Masahiko
Synthesis (Germany), 2012 , vol. 44, # 14 art. no. SS-2012-F0295-OP, p. 2209 - 2216
反应条件
pyridine; potassium tert-butylate; iodine
T=90°C; 2 h;
参考文献
Siddappa, Chandrappa; Kambappa, Vinaya; Umashankara, Muddegowda; Rangappa, Kanchugarakoppal S.
Tetrahedron Letters, 2011 , vol. 52, # 42 p. 5474 - 5477
反应条件
oxygen; copper diacetate in dimethyl sulfoxide
T=130°C; 26 h; Sealed tube;
参考文献
Song, Qiuling; Feng, Qiang; Zhou, Mingxin
Organic Letters, 2013 , vol. 15, # 23 p. 5990 - 5993
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide
T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942
反应条件
sodium dithionite in dimethyl sulfoxide
T=80°C; 4 h; Molecular sieve;
参考文献
Wang, Zhanglin; Tang, Riyuan; Xiao, Qin
Chinese Journal of Chemistry, 2011 , vol. 29, # 2 p. 314 - 320
反应条件
in water; N,N-dimethyl-formamide
3 h; Sonographic reaction;
参考文献
Zheng, Shijun
Patent: US2011/196158 A1, 2011 ;
Location in patent: Page/Page column 9-10 ;
反应条件
1: Br2 / AlCl3 / 1,2-dichloro-ethane / 40 - 45 °C
2: 82 percent / dimethylsulfoxide / 0.5 h / 200 °C
View Scheme
参考文献
Chen, Lianqing; Yang, Chuluo; Li, Suyue; Qin, Jingui
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 2 p. 317 - 322
反应条件
1: chloro-trimethyl-silane / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
2: N,N-dimethyl-formamide; water / 3 h / Sonographic reaction
View Scheme
参考文献
Zheng, Shijun
Patent: US2011/196158 A1, 2011 ;
反应条件
[bis(acetoxy)iodo]benzene; palladium diacetate; acetic acid
T=110°C; 4.5 h; regioselective reaction;
参考文献
Banerjee, Arghya; Bera, Anupam; Guin, Srimanta; Rout, Saroj Kumar; Patel, Bhisma K.
Tetrahedron, 2013 , vol. 69, # 9 p. 2175 - 2183
