1-(2-苯并噻唑基)-4-溴苯合成路线 (共 28 条)
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide; toluene 2 h; Reflux;
参考文献
Weekes, Ashley A.; Frydrych, Jan; Westwell, Andrew D.
Synthetic Communications, 2013 , vol. 43, # 19 p. 2656 - 2662
反应条件
(R)-(+)-1,1'-binaphthyl-2,2'-diamine; caesium carbonate; copper dichloride in acetonitrile T=110°C; 48 h; Inert atmosphere;
参考文献
Jaseer; Prasad; Dandapat, Arpan; Sekar, Govindasamy
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 5009 - 5012
反应条件
anhydrous phosphorus trichloride in toluene
反应条件
pyridine; anhydrous iron chloride; sodium peroxodisulphate in dimethyl sulfoxide T=80°C; 3 h; Inert atmosphere;
参考文献
Wang, Haibo; Wang, Lu; Shang, Jinsai; Li, Xing; Wang, Haoyuan; Gui, Jie; Lei, Aiwen
Chemical Communications, 2012 , vol. 48, # 1 p. 76 - 78
反应条件
tetrabutylammomium bromide; silver(I) acetate; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=120°C; 18 h; Molecular sieveInert atmosphere;
参考文献
Saha, Debasree; Adak, Laksmikanta; Ranu, Brindaban C.
Tetrahedron Letters, 2010 , vol. 51, # 42 p. 5624 - 5627
反应条件
1,10-phenanthroline; CuCl2·2H2O; potassium carbonate; sulfur in water T=100°C; 24 h;
参考文献
Deng, Hang; Li, Zhengkai; Ke, Fang; Zhou, Xiangge
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4840 - 4843
反应条件
[Fe(phthalocyanine)]; sodium t-butanolate in toluene T=120°C; 36 h; Inert atmosphere;
参考文献
Bala, Manju; Verma, Praveen Kumar; Sharma, Upendra; Kumar, Neeraj; Singh, Bikram
Green Chemistry, 2013 , vol. 15, # 6 p. 1687 - 1693
反应条件
samarium; titanium tetrachloride in tetrahydrofuran T=40°C; 0.166667 h; Inert atmosphere;
参考文献
Shi, Da-Qing; Rong, Shao-Feng; Dou, Guo-Lan
Synthetic Communications, 2010 , vol. 40, # 15 p. 2302 - 2310
反应条件
palladium diacetate; copper (II) acetate monohydrate in 1,4-dioxane; diethylene glycol dimethyl ether T=120°C; 24 h; sealed vessel;
参考文献
Chen, Ru; Liu, Saiwen; Liu, Xinhua; Yang, Luo; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7675 - 7679
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942