1-(2-苯并噻唑基)-4-溴苯合成路线 （共 28 条）
反应条件
1: in water; dimethyl sulfoxide T=100°C; 1 h; Inert atmosphere; 2: With dipotassium peroxodisulfate 3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091
反应条件
toluene-4-sulfonic acid T=112 - 114°C; 0.0333333 h; microwave irradiation;
参考文献
Paul, Satya; Gupta, Mukta; Gupta, Rajive
Synthetic Communications, 2002 , vol. 32, # 23 p. 3541 - 3547
反应条件
1: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C 2: CuCl2·2H2O; 1,10-phenanthroline; potassium carbonate; sulfur / water / 24 h / 100 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 16 p. 4840 - 4843
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux 2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C View Scheme
参考文献
Tetrahedron, , vol. 70, # 2 p. 245 - 250
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux 2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C View Scheme
参考文献
Tetrahedron, , vol. 70, # 2 p. 245 - 250
反应条件
potassium fluoride; C94H134O4P2Pd2; silver fluoride in cyclohexane T=90°C; 14 h; Sealed tube;
参考文献
Journal of the American Chemical Society, , vol. 136, # 10 p. 3792 - 3795
反应条件
potassium fluoride; C94H134O4P2Pd2; silver fluoride in cyclohexane
T=90°C; 14 h; Sealed tube;
参考文献
Lee, Hong Geun; Milner, Phillip J.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2014 , vol. 136, # 10 p. 3792 - 3795
反应条件
2-phenyl-1H-imidazole; potassium carbonate; palladium dichloride in N,N-dimethyl-formamide
T=120°C; Suzuki-Miyaura coupling; 20 h; Inert atmosphere;
参考文献
Dhayalan, Vasudevan; Hayashi, Masahiko
Synthesis (Germany), 2012 , vol. 44, # 14 art. no. SS-2012-F0295-OP, p. 2209 - 2216
