1,2-二(2-甲基-2-丙基)-3-二氮杂环丙二酮合成路线 （共 7 条）
反应条件
1,2-di-tert-butylhydrazine in benzene
参考文献
Greene,F.D. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 8 p. 2263 - 2269
反应条件
1: 2-methyl-propan-2-ol 2: aq. HCl View Scheme
参考文献
Greene,F.D. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 8 p. 2254 - 2262
反应条件
tetracarbonylnickel(0) in N,N-dimethyl-formamide T=70°C; Cycloaddition; 1 h;
参考文献
Komatsu, Mitsuo; Tamabuchi, Satoshi; Minakata, Satoshi; Ohshiro, Yoshiki
Heterocycles, 1999 , vol. 50, # 1 p. 67 - 70
反应条件
tetracarbonylnickel(0) in N,N-dimethyl-formamide T=70°C; Cycloaddition; 10 h;
参考文献
Komatsu, Mitsuo; Tamabuchi, Satoshi; Minakata, Satoshi; Ohshiro, Yoshiki
Heterocycles, 1999 , vol. 50, # 1 p. 67 - 70
反应条件
tetracarbonylnickel(0) in N,N-dimethyl-formamide
T=70°C; Cycloaddition; 1 h;
参考文献
Komatsu, Mitsuo; Tamabuchi, Satoshi; Minakata, Satoshi; Ohshiro, Yoshiki
Heterocycles, 1999 , vol. 50, # 1 p. 67 - 70
反应条件
tetracarbonylnickel(0) in N,N-dimethyl-formamide
T=70°C; Cycloaddition; 10 h;
参考文献
Komatsu, Mitsuo; Tamabuchi, Satoshi; Minakata, Satoshi; Ohshiro, Yoshiki
Heterocycles, 1999 , vol. 50, # 1 p. 67 - 70
反应条件
α,α-diphenylacetonitrile; lithium diisopropyl amide
1) THF, -70 deg C 2) a) THF, -70 deg C b) to reflux; Yield given. Multistep reaction;
参考文献
Komatsu; Yagii; Ohshiro
Tetrahedron Letters, 1990 , vol. 31, # 37 p. 5327 - 5330
