2-[Β(2-噻吩基)乙烯基]苯甲酸合成路线 （共 6 条）
反应条件
potassium hydroxide in tetrahydrofuran T=20°C; Wittig-Horner reaction; 0.25 h;
参考文献
Murty; Ramalingam; Sabitha; Yadav
Heterocyclic Communications, 2001 , vol. 7, # 5 p. 449 - 454
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; 12 h;
参考文献
Murty; Ramalingam; Sabitha; Yadav
Heterocyclic Communications, 2001 , vol. 7, # 5 p. 449 - 454
反应条件
1: 80 percent / 5 h / 150 °C 2: 80 percent / potassium hydroxide / tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Murty; Ramalingam; Sabitha; Yadav
Heterocyclic Communications, 2001 , vol. 7, # 5 p. 449 - 454
反应条件
1: 82 percent / N-bromosuccinimide; benzoylperoxide / CCl4 / 2 h / Heating 2: 80 percent / 5 h / 150 °C 3: 80 percent / potassium hydroxide / tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Murty; Ramalingam; Sabitha; Yadav
Heterocyclic Communications, 2001 , vol. 7, # 5 p. 449 - 454
反应条件
sodium hydroxide; hydrogen; palladium on activated charcoal T=100°C; P=15200 Torr; 12 h;
参考文献
Murty; Ramalingam; Sabitha; Yadav
Heterocyclic Communications, 2001 , vol. 7, # 5 p. 449 - 454
反应条件
1: 80 percent / aq. sodium hydroxide; hydrogen / Pd/C / 12 h / 100 °C / 15200 Torr 2: 60 percent / polyphosphoric acid / xylene / 2 h / 120 - 130 °C View Scheme
参考文献
Murty; Ramalingam; Sabitha; Yadav
Heterocyclic Communications, 2001 , vol. 7, # 5 p. 449 - 454
