3,6-二甲基-1H-嘧啶-2,4-二酮合成路线 （共 35 条）
参考文献
Bachstez
Chemische Berichte, 1931 , vol. 64, p. 2686
反应条件
sodium hydroxide
40 h; Heating;
参考文献
Grahner; Winiwarter; Lanzner; Muller
Journal of Medicinal Chemistry, 1994 , vol. 37, # 10 p. 1526 - 1534
反应条件
sodium in N,N-dimethyl-formamide; isopropyl alcohol
参考文献
Reznik, V. S.; Shvetsov, Yu. S.; Giniyatullin, R. Kh.; Samatova, N. A.; Podzigun, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, p. 1666 - 1672
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 10 p. 2349 - 2356
反应条件
1: 65 percent / 15percent aq. NaOH / 40 h / Heating
2: 79 percent / HNO3, H2SO4 / 0 - 5 °C
3: 66 percent / dimethylformamide / 2 h / Ambient temperature
4: 36 percent / H2 / 10percent Pd/C / methanol / 2 h / 760 Torr / Ambient temperature
View Scheme
参考文献
Grahner; Winiwarter; Lanzner; Muller
Journal of Medicinal Chemistry, 1994 , vol. 37, # 10 p. 1526 - 1534
反应条件
1: 65 percent / 15percent aq. NaOH / 40 h / Heating
2: 79 percent / HNO3, H2SO4 / 0 - 5 °C
View Scheme
参考文献
Grahner; Winiwarter; Lanzner; Muller
Journal of Medicinal Chemistry, 1994 , vol. 37, # 10 p. 1526 - 1534
