2,5,8,11-四氧杂十四碳-13-烯合成路线 （共 3 条）
反应条件
1: 2-[2-(2-methoxy-ethoxy)-ethoxy]-ethanol With sodium hydride in N,N-dimethyl-formamide; mineral oil T=0°C; 0.0833333 h; Inert atmosphere; 2: 3-chloroprop-1-ene in N,N-dimethyl-formamide; mineral oil T=0°C; 0.666667 h;
参考文献
ISIS INNOVATION LIMITED
Patent: US2012/178913 A1, 2012 ;
Location in patent: Page/Page column 12 ;
反应条件
1: 2-[2-(2-methoxy-ethoxy)-ethoxy]-ethanol With sodium hydride in tetrahydrofuran T=0°C; 2 h; 2: allyl bromide in tetrahydrofuran
参考文献
Kaplanek, Robert; Paleta, Oldrich; Ferjentsikova, Ivana; Kodicek, Milan
Journal of Fluorine Chemistry, 2009 , vol. 130, # 3 p. 308 - 316
反应条件
in ethyl acetate; toluene
参考文献
Northeastern University
Patent: US4778909 A1, 1988 ;
