(R)-(+)-叔丁基亚磺酰胺合成路线 (共 15 条)
反应条件
ammonia; lithium; iron nitrate (III) in tetrahydrofuran T=-78°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 124, # 27 p. 7880 - 7881
反应条件
acetic acid in methanol T=40°C; 20 h;
参考文献
Journal of the American Chemical Society, , vol. 125, # 37 p. 11276 - 11282
反应条件
acetic acid in methanol T=40°C; 20 h;
参考文献
Journal of the American Chemical Society, , vol. 125, # 37 p. 11276 - 11282
反应条件
lithium amide; ammonia T=-78°C; 0.25 h;
参考文献
Journal of the American Chemical Society, , vol. 120, # 32 p. 8011 - 8019
反应条件
ammonia; lithium; ammonium chloride T=-40°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 120, # 32 p. 8011 - 8019
反应条件
1: With bis(acetylacetonate)oxovanadium; (1S,2R)-1-(3,5-di-tert-butyl-2-hydroxybenzylideneamino)-2,3-dihydro-1H-inden-2-ol; dihydrogen peroxide in acetone T=0°C; 2: With ammonia; lithium; iron nitrate (III) in tetrahydrofuran T=-78°C;
参考文献
Organic Letters, , vol. 5, # 8 p. 1317 - 1320
反应条件
lithium amide; ammonia in tetrahydrofuran T=-78°C;
参考文献
Tetrahedron, , vol. 61, # 26 p. 6386 - 6408
反应条件
ammonia; lithium; iron nitrate (III) T=-78°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 24 p. 8533 - 8536
参考文献
US2014/80819 A1, ;
Page/Page column ;
反应条件
ammonia; sodium; iron nitrate (III) in CPME T=-48 - 20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Journal of Organic Chemistry, , vol. 74, # 7 p. 2646 - 2650