反应条件
Stage #1: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '110354', constants.ctx, '0')">4-(N,N-dimethlyamino)pyridine</a>; <a href="#" onclick="return RXDsubstances(event, this, '5764110', constants.ctx, '0')">1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0 - 20°C; <br />Stage #2: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '11343078', constants.ctx, '0')">sodium tetrahydroborate</a>; <a href="#" onclick="return RXDsubstances(event, this, '506007', constants.ctx, '0')">acetic acid</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=20°C; 48 h; <br />Stage #3: <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />6 h; Reflux; <br />
参考文献
Claudon, Paul; Violette, Aude; Lamour, Karen; Decossas, Marion; Fournel, Sylvie; Heurtault, Beatrice; Godet, Julien; Mely, Yves; Jamart-Gregoire, Brigitte; Averlant-Petit, Marie-Christine; Briand, Jean-Paul; Duportail, Guy; Monteil, Henri; Guichard, Gilles Angewandte Chemie - International Edition, 2010 , vol. 49, # 2 p. 333 - 336
