二甲基(2-噻吩基)硅烷醇合成路线 (共 9 条)
反应条件
air; water; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in acetonitrile T=25°C; 0.166667 h;
参考文献
Lee; Ko; Chang
Journal of the American Chemical Society, 2000 , vol. 122, # 48 p. 12011 - 12012
反应条件
1: thiophene With n-butyllithium in diethyl ether; hexane T=-71 - 20°C; 2: cyclo-(Me2SiO)3 in diethyl ether; hexane T=-71 - 20°C;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455
反应条件
sodium hydride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in toluene T=80°C; 24 h;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455
反应条件
sodium hydride; tri(tert-butyl)phosphine palladium complex in toluene T=50°C; 3 h;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455
反应条件
sodium hydride; tri(tert-butyl)phosphine palladium complex in toluene T=50°C; 3 h;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455
反应条件
sodium hydride; tri(tert-butyl)phosphine palladium complex in toluene T=50°C; 3 h;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455
反应条件
sodium hydride; tri(tert-butyl)phosphine palladium complex in toluene T=50°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 4 p. 1440 - 1455
反应条件
sodium hydride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in toluene
T=20°C; 3 h;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455
反应条件
sodium hydride; tri(tert-butyl)phosphine palladium complex in toluene
T=50°C; 3 h;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455