反应条件
1.1: t-BuLi / tetrahydrofuran; pentane / 0.5 h / -78 - 0 °C 1.2: tetrahydrofuran; pentane / -78 - 25 °C 2.1: 17.5 g / aq. Jones' reagent / tetrahydrofuran / 18 h / 25 °C 3.1: tetrahydrofuran / 1.25 h / 0 - 25 °C 4.1: Bu2Mg / tetrahydrofuran; pentane / -78 - 25 °C 4.2: tetrahydrofuran / 25 °C 5.1: 4-acetamidobenzenesulfonyl azide; Et3N / acetonitrile / 25 °C View Scheme
参考文献
Hodgson, David M.; Stupple, Paul A.; Pierard, Francoise Y. T. M.; Labande, Agnes H.; Johnstone, Craig
Chemistry - A European Journal, 2001 , vol. 7, # 20 p. 4465 - 4476
